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Set-Up
for Operating:
The pressure
gauge has been calibrated to +/- 1/4 pound psi at the factory prior
to shipment of the instrument. If, after a period of use, there
is a question of gauge accuracy the following checks should be performed
on the gauge:
The gauge should
be checked and calibrated using any of the following instruments:
- A Zahm &
Nagel Series #8000 Gauge Tester
- A Dead Weight
Tester
- A calibrated
Test Gauge Digital
The most accurate
range of the gauge is the mid-range and the needle should be set
in this area. To re-set the needle, remove the face cover and insert
a small screwdriver into the slotted brass screw located at the
5 o'clock position of the gauge. Turn the screw-driver clockwise
or counterclockwise to match the pressure established on one of
the above testing devices. A "Zero Zone" is located on the gauge
and the needle may rest in any area of this zone and still be in
calibration. Do not attempt to calibrate the gauge in this zone.
Gauges that are out of calibration may be returned to Zahm & Nagel
for re-calibration.
The thermometer
liquid column may become separated due to rough handling. The column
may be re-joined by following the instruction sheet on "Separated
Columns" that is shipped with this instrument. These instruction
sheets are also available from Zahm & Nagel Co. upon request. Replacement
thermometers are also available from Zahm & Nagel Co.
WARNING:
OPERATOR MUST WEAR EYE PROTECTION WHILE OPERATING THIS INSTRUMENT.
OPERATING:
Before using
the Volume Meter, rinse the inside with cold water. This will help
prevent gas bubbles from adhering to the internal surfaces of the
Volume Meter when it is being filled.
- Close the
inlet valve (2035) and the bleeder valve (3003).
- Open the
overflow valve (2002) and pump the aspirator bulb (1042)
until a pressure of 10 psi is indicated on the gauge (2013).
- Close the
overflow valve (2002) and allow the instrument to stand
for several minutes. If the gauge shows any pressure drop, a leak
is indicated and may be detected by applying a soapy water solution
to the various fittings and the condition corrected.
- Attach the
Volume Meter to the trycock on the tank by turning the U-bolt
nut (2045) on the clamping device (2037) to its
most open position (out) and place the Volume Meter over the boss
of the trycock.
- Spin the
U-bolt nut closed to seal the Volume Meter tightly to the trycock.
- Make sure
the bleeder valve on the pressure gauge is closed and then open
both the inlet (2035) and the overflow (2002) valves
on the Volume Meter.
- Pump counter-pressure
into the Volume Meter with the aspirator bulb. The counter-pressure
should be equal or slightly less than the pressure of the tank,
plus the hydrostatic head pressure of the beer above the trycock.
For example: if the tank pressure is 8 psi and the beer level
is 6 feet above the trycock or approximately 3 psi pressure, 11psi
counter-pressure should be established in the Volume Meter.
- Close the
overflow valve (2002) and remove the aspirator bulb (1042)
from the Volume Meter.
- Open the
trycock on the beer tank to allow beer to flow into the Volume
Meter. However, due to the counter-pressure established in the
Volume Meter, the beer will be prevented from flowing into the
instrument. In order to establish flow, slightly open the overflow
valve (2002) and allow the pressure to drop slowly in the
Volume Meter. To avoid too rapid a release of pressure, which
would have a disturbing effect on the beer flowing into the Volume
Meter, let the pressure gauge act as a guide. A pressure drop
of ½ to I psi will allow the Volume Meter to fill properly. When
the filling operation is properly performed, the beer will quietly
fill the Volume Meter with a minimum of released gas. It is advisable
to have the Volume Meter cooling in the cellar a short time before
making the test. The beer is now allowed to completely fill the
overflow tube (2001). A small amount of beer is allowed
to escape to remove free gas bubbles.
- Close the
overflow valve (2002) and also the inlet valve (2035).
- Close the
trycock on the beer tank and remove the Volume Meter by releasing
the U-bolt on the clamping device (2037).
- Remove a
small definite amount of beer from the Volume Meter to allow proper
agitation and to make possible the equilibrium condition between
free and dissolved gas upon which the operation of the instrument
is based. To remove the beer, open the bleeder valve (3003)
and allow the beer to flow out of the bleeder valve until it reaches
the indicated beer level line on the sight glass (2006).
It is best to release the beer in three or more portions, and
after each release hold the Volume Meter vertically by the handles
and rotate the Volume Meter in a circle while keeping the sight
glass (2006) at a fixed point. This motion will bring the
gas that will be released when each portion of the beer is removed
up into the sight glass so that the liquid level can be more accurately
adjusted to the beer level line. A level of 1/16" above or below
the line will cause only a minor error and, unless most exact
results are desired, such an adjustment will be sufficiently accurate.
If beers of low CO2 content are to be tested, it may be necessary
to warm the sample to obtain sufficient pressure to bleed off
the required amount.
- Now after
the beer level has been adjusted to the line described, hold the
Volume Meter by the two handles in a horizontal position and vigorously
agitate the instrument. This agitation causes the rapid establishment
of equilibrium between the free and dissolve gas. Under conditions
of equilibrium the number of volumes of gas in a given beer will
be in constant relationship to the temperature and pressure conditions.
That is to say, a beer having a fixed volume of CO2 gas in solution
will show the same pressure at a given temperature and conversely,
the same temperature at a given pressure. When the temperature
and pressure remain constant these indications are referred to
the chart from which the number of volumes of CO2 gas at zero
degrees C., 760mm pressure per volume of beer is stated. When
making the pressure reading, always hold the Volume Meter in a
vertical position so as to obtain accurate indications. After
one set of readings has been taken, agitate the instrument again
and check the temperature and pressure indicated. There should
be no material difference if the temperature has remained constant.
The chart furnished with the Volume Meter was compiled after extensive
laboratory research. Samples were taken from a tank containing
carbonated beer at equilibrium with undissolved gas. One set of
these samples was tested with the Volume Meter using the method
previously described while the other set was analyzed by exact
chemical methods. The result of these analyses were plotted against
the temperatures and pressures as indicated by the Volume Meter
in testing each duplicate sample. Hence, the chart gives the number
of volumes of CO2 gas dissolved per volume of beer as contained
in the tank from which the sample was taken and does not indicate
the number of volumes of gas dissolved in the sample contained
in the Volume Meter. This is due to having liberated 3% of the
dissolved gas to replace the beer in the space above the beer
level line in the Volume Meter. When the Volume Meter is used
at high altitudes, or when the barometer is low, or if very exact
results are desired, the pressure gauge reading should be corrected
before reference to the chart is made. Deduct 0.2 psi for every
10mm mercury indicated by the barometer below the standard condition
of 760mm mercury. If the percentage of weight of CO2 gas is desired,
the following formula may be used:
Volume of CO2 x O.197
Specific Gravity of Beer
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= % CO2 weight |
NOTE: The Volume Meter chart gives solubility of CO2 gas
in average beer, and will be found to give lower reading than
charts based on solubility in water.
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